儀器校正方式和步驟-深圳市慧聰源環(huán)?？萍加邢薰?/title> <link rel="stylesheet" type="text/css" href="/skins/270528/css/style.css"> <script src="/skins/270528/js/jquery-3.6.0.min.js"></script> <link rel="shortcut icon" href="/skins/270528/favicon.ico">  <script type="text/javascript"> document.addEventListener("touchstart", function () { }, true); </script>  <script language="javascript" type="text/javascript"> var nav= '5'; </script>  <script type="application/ld+json"> { "@context": "https://ziyuan.baidu.com/contexts/cambrian.jsonld", "@id": "http:///szhcy-Article-1920830/", "title": "儀器校正方式和步驟", "pubDate": "2019-08-03T16:40:58", "upDate": "2019-08-03T16:40:58" }</script> <script language="javaScript" src="/js/JSChat.js"></script><script language="javaScript">function ChatBoxClickGXH() { DoChatBoxClickGXH('https://chat.chem17.com',262687) }</script><script> (function(){ var bp = document.createElement('script'); var curProtocol = window.location.protocol.split(':')[0]; if (curProtocol === 'https') { 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點擊次數(shù)：3265</div> <div id="ht5bhtv" class="NyNewsdetail_con"> <p><span style="font-family:宋體">儀器校正方式</span></p><p><span style="font-family:宋體"> 對于</span>pH<span style="font-family:宋體">值的校準(zhǔn)，儀器提供了一點和兩點自動或手動校準(zhǔn)。自盡校準(zhǔn)可以識別對應(yīng)所選擇的緩沖溶液數(shù)據(jù)表，并且可以在穩(wěn)定之后自動校準(zhǔn)電極。手動校準(zhǔn)將</span><strong>pH</strong><strong><span style="font-family:宋體">電極</span></strong><span style="font-family:宋體">放置到任意一個已知值的樣品或緩沖溶液中，然后將該已知數(shù)值輸入控制器中。手動校準(zhǔn)時所使用的樣品值可以通過實驗室分析或比較讀數(shù)的方法確定。</span></p><p><span style="font-family:宋體">校準(zhǔn)步驟</span></p><p><span style="font-family:宋體"> 使用新的電極時，為了獲得好的效果，一定要在校準(zhǔn)之前讓樣品流過測量室至少</span>10h<span style="font-family:宋體">。為了能對</span><strong>pH</strong><strong><span style="font-family:宋體">電極</span></strong><span style="font-family:宋體">進(jìn)行校準(zhǔn)，必須使用兩點校準(zhǔn)方法。建議使用</span>pH<span style="font-family:宋體">值為</span>4<span style="font-family:宋體">和</span>7<span style="font-family:宋體">的緩沖溶液。對于次標(biāo)準(zhǔn)化，需要使用</span>pH<span style="font-family:宋體">值為</span>7<span style="font-family:宋體">的緩沖溶液，對于電極斜率的校準(zhǔn)，需要使用</span>pH<span style="font-family:宋體">值為</span>4<span style="font-family:宋體">（或</span>pH<span style="font-family:宋體">值為</span>l0<span style="font-family:宋體">）的緩沖溶液。使用方法如下。</span> </p><p> a. <span style="font-family:宋體">將流通池的螺釘放置在合適的位置上，擰開流通池，見圖</span>2-18<span style="font-family:宋體">。 </span><img src="http://img71.chem17.com/9/20190803/637004455779793507447.png" style="height:401px; width:259px" /></p><p style="margin-left:18pt">b. <span style="font-family:宋體">清空流通池中的水，并使用蒸餾水進(jìn)行潤洗。</span></p><p style="margin-left:18pt">c. <span style="font-family:宋體">使用蒸餾水潤洗電極。</span></p><p style="margin-left:18pt">d. <span style="font-family:宋體">使用</span>pH<span style="font-family:宋體">值為</span>7<span style="font-family:宋體">的緩沖溶液填充流通池，并重新裝配流通池。注意：一定要使用制備的緩沖溶。</span>,</p><p style="margin-left:18pt">e. <span style="font-family:宋體">按照儀器指示進(jìn)行兩點自動校準(zhǔn)方法來校準(zhǔn)點。</span></p><p style="margin-left:18pt">f. <span style="font-family:宋體">拆除流通池，清空種緩沖溶液，并使用蒸餾水潤洗流通池和電極。</span></p><p style="margin-left:18pt">g. <span style="font-family:宋體">使用</span>pH<span style="font-family:宋體">值為</span>4 (<span style="font-family:宋體">或</span>pH<span style="font-family:宋體">值為</span>10)<span style="font-family:宋體">的緩沖溶液填充流通池，并重新裝配。</span></p><p style="margin-left:18pt">h. <span style="font-family:宋體">按照儀器指示的兩點自動校準(zhǔn)方法來校準(zhǔn)第二點。</span></p><p style="margin-left:18pt">i. <span style="font-family:宋體">拆除流通池，清空第二種緩沖溶液，并使用蒸餾水潤洗流通池和電極，重新安裝流通池。</span></p><p style="margin-left:18pt">j. <span style="font-family:宋體">將樣品流速調(diào)節(jié)到</span>100-300mL/min<span style="font-family:宋體">，樣品流過裝置至少</span>1h<span style="font-family:宋體">。</span></p><p style="margin-left:18pt">k. <span style="font-family:宋體">使用合格的標(biāo)準(zhǔn)測定儀進(jìn)行溢流方法樣品測量。</span></p><p style="margin-left:18pt">l. <span style="font-family:宋體">將測定儀的讀數(shù)與控制器上的讀數(shù)進(jìn)行比較。如果讀數(shù)有所不同，在控制器上進(jìn)行單點校準(zhǔn)，這樣控制器的讀數(shù)可以與標(biāo)準(zhǔn)測定儀的讀數(shù)一致。</span></p> </div> <div id="fd5tlj3" class="ly_PrevNext"> <ul> <li>上一篇：<a href="/szhcy-Article-1920835/">水污染源在線監(jiān)測系統(tǒng)運(yùn)行與考核技術(shù)規(guī)范（試行）</a></li> <li>下一篇：<a href="/szhcy-Article-1920300/">克服和改善純水PH值的方法</a></li> </ul> </div> </div>   <div id="nhvdfrr" class="foot_box"> <div id="7zd33np" class="foot_t"> <div id="5tnlpbb" class="w1200"> <a href="/">網(wǎng)站首頁</a>　|　<a href="/aboutus.html">關(guān)于我們</a>　|　<a href="/products.html">產(chǎn)品中心</a>　|　<a href="/news.html">新聞動態(tài)</a>　|　<a href="/article.html">技術(shù)文章</a>　|　<a href="/honor.html">榮譽(yù)資質(zhì)</a>　|　<a href="/order.html" target="_blank">在線留言</a>　|　<a href="/contact.html">聯(lián)系我們</a> <span><a href="javascript:;" class="toTop"></a></span> </div> </div> <div id="z5fl3n3" class="foot_b"> <div id="rdd5p3x" class="w1200"> <div id="xhj3rft" class="f_b_t clear"> <div 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